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Volume 38 Issue 6
Nov 2024
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Chinese Journal of High Pressure Physics  > 2024  >  38(6): 063401.
ZHANG Ruike, GUO Rui’ang, XIAO Xiong, HE Duanwei. Measurement of the Melting Point of Hexagonal Boron Nitride under Pressures below 5 GPa[J]. Chinese Journal of High Pressure Physics, 2024, 38(6): 063401. doi: 10.11858/gywlxb.20240813
Citation: ZHANG Ruike, GUO Rui’ang, XIAO Xiong, HE Duanwei. Measurement of the Melting Point of Hexagonal Boron Nitride under Pressures below 5 GPa[J]. Chinese Journal of High Pressure Physics, 2024, 38(6): 063401. doi: 10.11858/gywlxb.20240813
shu

Measurement of the Melting Point of Hexagonal Boron Nitride under Pressures below 5 GPa

doi: 10.11858/gywlxb.20240813

  • Institute of Atomic and Molecular Physics, Sichuan University, Chengdu 610065, Sichuan, China

  • Received Date: 17 May 2024
  • Rev Recd Date: 31 May 2024
    • Available Online: 02 Sep 2024
  • Issue Publish Date: 05 Dec 2024
    Abstract
  • In this study, a flash-heating device was designed and assembled to achieve instantaneous discharge heating of samples under high pressure in the DS 6×14 MN domestic hinged six-anvil large chamber press. By combining large chamber static high pressure and instantaneous discharge heating technologies, the melting state of crystals has been determined by the nucleation and growth characteristics during solidification. The melting behavior of h-BN powder crystal under high pressure was studied by instantaneous discharge heating treatment. Using scanning electron microscopy (SEM), the microstructures of samples obtained by high-pressure instantaneous discharge heating treatment was analyzed in order to assess the melting state of h-BN crystals. It was determined that the melting points of h-BN under 3.4 and 4.3 GPa are (4251±150) K and (4531±200) K, respectively. These results are beneficial for exploring the applications of h-BN and revising the existed temperature-pressure phase diagram of boron nitride.

     

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