knowledge of professional and technical personnel Notice on the organization of advanced research class on high-pressure science and new materials of engineering
Volume 36 Issue 1
Jan 2022
Turn off MathJax
Article Contents
Chinese Journal of High Pressure Physics  > 2022  >  36(1): 011201.
ABLIZ Matursun, ANWAR Hushur, XIE Cuihuan, QI Wenming. High Pressure Raman Spectroscopic Study of PbCO3 in Different Pressure Transmitting Medium[J]. Chinese Journal of High Pressure Physics, 2022, 36(1): 011201. doi: 10.11858/gywlxb.20210813
Citation: ABLIZ Matursun, ANWAR Hushur, XIE Cuihuan, QI Wenming. High Pressure Raman Spectroscopic Study of PbCO3 in Different Pressure Transmitting Medium[J]. Chinese Journal of High Pressure Physics, 2022, 36(1): 011201. doi: 10.11858/gywlxb.20210813
shu

High Pressure Raman Spectroscopic Study of PbCO3 in Different Pressure Transmitting Medium

doi: 10.11858/gywlxb.20210813

  • School of Physical Science and Technology, Xinjiang University, Urumqi 830046, Xinjiang, China

  • Received Date: 15 Jun 2021
  • Rev Recd Date: 06 Jul 2021
    Abstract
  • Using diamond anvil cell (DAC) technique and Raman spectroscopy, we have studied the stability of PbCO3 at high pressure. Solid NaCl, mixture of methanol-ethanol-water (16∶3∶1) and methanol-ethanol (4∶1) were used as pressure transmitting medium. The highest pressure in this study reached up to 24.5, 25.0 and 67.0 GPa, respectively. It is found that PbCO3 undergoes three phase transitions at around 10, 15 and 30 GPa, respectively. In addition, the softening of the out of bending vibration mode belonging to ${\rm{CO}}_3^{2-} $ group was observed. By comparison with the Grüneisen parameters ($\gamma $) of PbCO3 in different pressure-transfer media, the phase transition mechanism is slightly different, and the influence of pressure on lattice vibration is greater than that of ${\rm{CO}}_3^{2-} $ group, which is attributed to the larger distance of the Pb2+—O bond. PbCO3 did not decompose or amorphized in the pressure range of 67.0 GPa, the highest pressure reached in this study. The observed PbCO3-Ⅳ phase above 30.0 GPa is stable up to 67.0 GPa.

     

    • FullText(HTML)
  • loading
    • References(22)
  • [1]
    MCGETCHIN T R, BESANCON J R. Carbonate inclusions in mantle-derived pyropes [J]. Earth and Planetary Science Letters, 1973, 18(3): 408–410. doi: 10.1016/0012-821X(73)90096-4
    [2]
    KUSHIRO I. Carbonate-silicate reactions at high presures and possible presence of dolomite and magnesite in the upper mantle [J]. Earth and Planetary Science Letters, 1975, 28(2): 116–120. doi: 10.1016/0012-821X(75)90218-6
    [3]
    宋文磊, 许成, 刘琼, 等. 火成碳酸岩的实验岩石学研究及对地球深部碳循环的意义 [J]. 地质论评, 2012, 58(4): 726–744. doi: 10.3969/j.issn.0371-5736.2012.04.014

    SONG W L, XU C, LIU Q, et al. Experimental petrological study of carbonatite and its significances on the earth deep carbon cycle [J]. Geological Review, 2012, 58(4): 726–744. doi: 10.3969/j.issn.0371-5736.2012.04.014
    [4]
    穆巴拉克 • 木里提江. 碳酸盐的高温高压稳定性及碳循环问题的研究 [D]. 乌鲁木齐: 新疆大学, 2019.

    MUBARAK M. Study on high pressure and high temperature stability of carbonate and deep Earth’s carbon cycle [D]. Urumqi: Xinjiang University, 2019.
    [5]
    SANTILLÁN J, WILLIAMS Q, KNITTLE E. Dolomite-Ⅱ: a high-pressure polymorph of CaMg(CO3)2 [J]. Geophysical Research Letters, 2003, 30(2): 1054. doi: 10.1029/2002GL016018
    [6]
    MINCH R, PETERS L, EHM L, et al. Evidence for the existence of a PbCO3-Ⅱ phase from high pressure X-ray measurements [J]. Zeitschrift für Kristallographie, 2010, 225(4): 146–152. doi: 10.1524/zkri.2010.1194
    [7]
    GAO J, WU X, QIN S, et al. Pressure-induced phase transformations of PbCO3 by X-ray diffraction and Raman spectroscopy [J]. High Pressure Research, 2016, 36(1): 1–15. doi: 10.1080/08957959.2015.1118475
    [8]
    CATALLI K, SANTILLÁN J, WILLIAMS Q. A high pressure infrared spectroscopic study of PbCO3-cerussite: constraints on the structure of the post-aragonite phase [J]. Physics and Chemistry of Minerals, 2005, 32(5/6): 412–417. doi: 10.1007/s00269-005-0010-9
    [9]
    LIN C C, LIU L G. High pressure phase transformations in aragonite-type carbonates [J]. Physics and Chemistry of Minerals, 1997, 24(2): 149–157. doi: 10.1007/s002690050028
    [10]
    MINCH R, DUBROVINSKY L, KURNOSOV A, et al. Raman spectroscopic study of PbCO3 at high pressures and tempera-tures [J]. Physics and Chemistry of Minerals, 2010, 37(1): 45–56. doi: 10.1007/s00269-009-0308-0
    [11]
    KAMINSKII A A, BOHATÝ L, RHEE H, et al. Cerussite, PbCO3: a new stimulated Raman scattering (SRS)-active crystal with high-order Stokes and anti-Stokes lasing: on the 50th anniversary of the discovery of stimulated Raman scattering [J]. Laser & Photonics Reviews, 2013, 7(3): 425–431. doi: 10.1002/lpor.201200123
    [12]
    ZHANG Y F, LIU J, QIN Z X, et al. A high-pressure study of PbCO3 by XRD and Raman spectroscopy [J]. Chinese Physics C, 2013, 37(3): 038001. doi: 10.1088/1674-1137/37/3/038001
    [13]
    MAO H K, BELL P M. Crystal-field effects in spinel: oxidation states of iron and chromium [J]. Geochimica et Cosmochimica Acta, 1975, 39(6/7): 865–866. doi: 10.1016/0016-7037(75)90032-0
    [14]
    徐济安. 金刚石砧高压实验中压强传递介质对实验的影响—镁铝榴石状态方程的实验测定 [J]. 高压物理学报, 1987, 1(2): 97–101. doi: 10.11858/gywlxb.1987.02.001

    XU J A. The effect of pressure transmitting medium on the high pressure experiments in diamond anvil cell (DAC): experimental measurement of the equation of state (EOS) of pyrope [J]. Chinese Journal of High Pressure Physics, 1987, 1(2): 97–101. doi: 10.11858/gywlxb.1987.02.001
    [15]
    张书霞. 高温高压合成实验所用传压介质的研究 [D]. 成都: 四川大学, 2006.

    ZHANG S X. A study on pressure mediums for high pressure and high temperature experiment [D]. Chengdu: Sichuan University, 2006.
    [16]
    KIRSCHNER S M, WATSON J K G. Sextic centrifugal distortion of tetrahedral molecules [J]. Journal of Molecular Spectroscopy, 1973, 47(2): 347–350. doi: 10.1016/0022-2852(73)90018-0
    [17]
    YANG J, DENG W, LI Q, et al. Strength enhancement of nanocrystalline tungsten under high pressure [J]. Matter and Radiation at Extremes, 2020, 5(5): 058401. doi: 10.1063/5.0005395
    [18]
    CHEN B. Exploring nanomechanics with high-pressure techniques [J]. Matter and Radiation at Extremes, 2020, 5(6): 068104. doi: 10.1063/5.0032600
    [19]
    LAVINA B, DERA P, DOWNS R T, et al. Siderite at lower mantle conditions and the effects of the pressure-induced spin-pairing transition [J]. Geophysical Research Letters, 2009, 36(23): L23306. doi: 10.1029/2009GL039652
    [20]
    LIANG W, YIN Y, LI Z M, et al. Single crystal growth, crystalline structure investigation and high-pressure behavior of impurity-free siderite (FeCO3) [J]. Physics and Chemistry of Minerals, 2018, 45(9): 831–842. doi: 10.1007/s00269-018-0965-y
    [21]
    穆巴拉克 • 木里提江, 艾尼瓦尔 • 吾术尔, 王静, 等. 碳酸钡在高温及高压下的相变行为 [J]. 材料导报, 2019, 33(12): 4062–4065.

    MOLUTJAN M, HUSHUR A, WANG J, et al. Phase transition of BaCO3 under high temperature and high pressure [J]. Materials Reports, 2019, 33(12): 4062–4065.
    [22]
    ONO S, KIKEGAWA T, OHISHI Y, et al. Post-aragonite phase transformation in CaCO3 at 40 GPa [J]. American Mineralogist, 2005, 90(4): 667–671. doi: 10.2138/am.2005.1610
    • Relative Articles
    • Supplements(0)
    • Cited By
  • 加载中

Catalog

    通讯作者: 陈斌, bchen63@163.com
    • 1. 

      沈阳化工大学材料科学与工程学院 沈阳 110142

    1. 本站搜索
    2. 百度学术搜索
    3. 万方数据库搜索
    4. CNKI搜索

    Figures(7)  / Tables(8)

    Get Citation
    PDF
    XML

    Article Metrics

    Article views(933) PDF downloads(53) Cited by()
    Proportional views
    Related

    Copyright©《高压物理学报》编辑部

    Tel:0816-2490042 E-mail:gaoya@caep.cn

    Shu ICP, 11011126 -2

    Supported by: Beijing Renhe Information Technology Co. Ltd support: info@rhhz.net  

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return