Synthesis of Pure Bulk Fe<sub>3</sub>C under High Temperature and High Pressure

YANG Jun; YANG Gang; CHEN Xing; ZHAO Bin; LENG Chunwei; LIU Xun; HUANG Haijun

doi:10.11858/gywlxb.20190715

Volume 33 Issue 4

Jul 2019

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Chinese Journal of High Pressure Physics > 2019 > 33(4): 043302.

BAI Hui, HUI Hu, YANG Bin, KONG Fang. Strain Response and Analysis of Pressure Vessels with Small Delamination Defects[J]. Chinese Journal of High Pressure Physics, 2021, 35(5): 054203. doi: 10.11858/gywlxb.20210717

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YANG Jun, YANG Gang, CHEN Xing, ZHAO Bin, LENG Chunwei, LIU Xun, HUANG Haijun. Synthesis of Pure Bulk Fe₃C under High Temperature and High Pressure[J]. Chinese Journal of High Pressure Physics, 2019, 33(4): 043302. doi: 10.11858/gywlxb.20190715

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Synthesis of Pure Bulk Fe₃C under High Temperature and High Pressure

doi: 10.11858/gywlxb.20190715

School of Science, Wuhan University of Technology, Wuhan 430070, China

Received Date: 18 Jan 2019
Rev Recd Date: 26 Mar 2019

Abstract

Abstract

Fe₃C (cementite) is a widely used material with excellent mechanical and magnetic properties; therefore the preparation method of Fe₃C has been widely concerned. In this paper, dense and high-purity bulk Fe₃C samples were prepared based on the solid-phase reaction of iron and carbon under high temperature and high pressure, and the influence of raw material type, particle size, sintering temperature, pressure, and holding time are investigated for the sintered samples. It shows that the densest samples were produced under the sintering pressure and temperature of 4 GPa and 1000 ̊C when the Fe and graphite particles were 9 ${\text{μ}}{\rm{m}}$ and 1.3 ${\text{μ}}{\rm{m}}$ respectively.
- Fe₃C,
- cubic anvil press,
- high temperature and high pressure,
- sintering

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References

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Synthesis of Pure Bulk Fe₃C under High Temperature and High Pressure

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