Volume 25 Issue 4
Apr 2015
Turn off MathJax
Article Contents
YANG Bin, LU Feng-Guo, ZHAO Xu-Dong, LIU Xiao-Yang. Use and Pressure Calibration of 1 000 Tons Walker Module High Pressure and High Temperature Apparatus[J]. Chinese Journal of High Pressure Physics, 2011, 25(4): 303-309 . doi: 10.11858/gywlxb.2011.04.003
Citation: YANG Bin, LU Feng-Guo, ZHAO Xu-Dong, LIU Xiao-Yang. Use and Pressure Calibration of 1 000 Tons Walker Module High Pressure and High Temperature Apparatus[J]. Chinese Journal of High Pressure Physics, 2011, 25(4): 303-309 . doi: 10.11858/gywlxb.2011.04.003

Use and Pressure Calibration of 1 000 Tons Walker Module High Pressure and High Temperature Apparatus

doi: 10.11858/gywlxb.2011.04.003
More Information
  • Corresponding author: LIU Xiao-Yang
  • Received Date: 24 Jan 2010
  • Rev Recd Date: 01 Apr 2010
  • Issue Publish Date: 15 Aug 2011
  • The two-stage 1 000 tons Walker module large-volume high temperature and high pressure apparatus can generate different pressures with different truncated edge lengths of anvils (12, 8, 6, and 4 mm). If tungsten carbide is chosen as an anvil, the maximum pressure obtained is above 20 GPa. The sample assemblies of Walker module apparatus are determined. The pressure calibration is performed by the fixed points of phase transitions method for different truncated edge lengths. The phase transition pressures of standard materials of pressure calibration (Bi, Tl, ZnTe, Pb, ZnS, GaAs) are achieved by measuring the resistance change with oil load under high pressure. The calibration curve of the sample pressure versus load is obtained, which provides exact information for future high pressure experiments using this apparatus.

     

  • loading
  • Jackson D D, Aracne-Ruddle C, Malba V, et al. Magnetic Susceptibility Measurements at High Pressure Using Designer Diamond Anvils [J]. Rev Sci Instrum, 2003, 74(4): 2467-2471.
    Xu J A, Mao H K, Bell P M. High-Pressure Ruby and Diamond Fluorescence: Observations at 0. 21 to 0. 55 Terapascal [J]. Science, 1986, 232(4756): 1404-1406.
    Ming L C, Bassett W A. Laser Heating in the Diamond Anvil Press up to 2000 ℃ Sustained and 3000 ℃ Pulsed at Pressures up to 260 Kilobars [J]. Rev Sci Instrum, 1974, 45(9): 1115-1118.
    Wang Y B, Durham W B, Getting I C, et al. The Deformation-DIA: A New Apparatus for High Temperature Triaxial Deformation to Pressures up to 15 GPa [J]. Rev Sci Instrum, 2003, 74(6): 3002-3011.
    Wang Y B. Combining the Large-Volume Press with Synchrotron Radiation: Applications to in-Situ Studies of Earth Materials under High Pressure and Temperature [J]. Earth Science Frontiers, 2006, 13(2): 1-37. (in Chinese)
    王雁宾. 地球内部物质物性的原位高温高压研究: 大体积压机与同步辐射源的结合 [J]. 地学前缘, 2006, 13(2): 1-37.
    Walker D, Carpenter M A, Hitch C M. Some Simplifications to Multianvil Devices for High Pressure Experiments [J]. Am Miner, 1990, 75(9-10): 1020-1028.
    Walker D. Lubrication, Gasketing, and Precision in Multianvil Experiments [J]. Am Miner, 1991, 76(7-8): 1092-1100.
    Ohtani E, Kagawa N, Shimomura O, et al. High-Pressure Generation by a Multiple Anvil System with Sintered Diamond Anvils [J]. Rev Sci Instrum, 1989, 60(5): 922-925.
    Ito E. Sintered Diamond Multi Anvil Apparatus and Its Application to Mineral Physics [J]. J Miner Petrol Sci, 2006, 101(3): 118-121.
    Tange Y, Irifune T, Funakoshi K I. Pressure Generation to 80 GPa Using Multianvil Apparatus with Sintered Diamond Anvils [J]. High Pressure Res, 2008, 28(3): 245-254.
    Onodera A. Octahedral-Anvil High-Pressure Devices [J]. High Temp High Press, 1987, 19: 579-609.
    Walter M J, Thibault Y, Wei K, et al. Characterizing Experimental Pressure and Temperature Conditions in Multi-Anvil Apparatus [J]. Can J Phys, 1995, 73(5-6): 273-286.
    Akimoto S, Manghnani M H. High-Pressure Research in Geophysics [M]. Tokyo: Center for Academic Publications Japan, 1982: 259.
    Ohtani E. Melting Relation of Fe2SiO4 up to about 200 kbar [J]. J Phys Earth, 1979, 27(3): 189-208.
    Takahashi E. Melting of a Dry Peridotite KLB-1 up to 14 GPa: Implications on the Origin of Peridotitic Upper Mantle [J]. J Geophys Res, 1986, 91(B9): 9367-9382.
    Bean V E, Akimoto S, Bell P M, et al. Another Step Toward an International Practical Pressure Scale: 2nd AIRAPT IPPS Task Group Report [J]. Physica, 1986, 139-140: 52-54.
    Homan C G. Phase Diagram of Bi up to 140 kbars [J]. J Phys Chem Solids, 1975, 36(11): 1249-1254.
    Ohtani A, Motobayashi M, Onodera A. Polymorphism of ZnTe at Elevated Pressure [J]. Phys Lett A, 1980, 75(5): 435-437.
    Ohtani A, Onodera A, Kawai N. Pressure Apparatus of Split-Octahedron Type for X-Ray Diffraction Studies [J]. Rev Sci Instrum, 1979, 50(3): 308-315.
    Kusaba K, Galoisy L, Wang Y B, et al. Determination of Phase Transition Pressures of ZnTe under Quasihydrostatic Conditions [J]. Pure Appl Phys, 1993, 141(2-4): 643-652.
    Piermarini G J, Block S. Ultrahigh Pressure Diamond-Anvil Cell and Several Semiconductor Phase Transition Pressures in Relation to the Fixed Point Pressure Scale [J]. Rev Sci Instrum, 1975, 46(8): 973-979.
    Onodera A, Ohtani A. Fixed Points for Pressure Calibration above 100 kbars Related to Semiconductor-Metal Transitions [J]. J Appl Phys, 1980, 51(5): 2581-2585.
  • 加载中

Catalog

    通讯作者: 陈斌, bchen63@163.com
    • 1. 

      沈阳化工大学材料科学与工程学院 沈阳 110142

    1. 本站搜索
    2. 百度学术搜索
    3. 万方数据库搜索
    4. CNKI搜索

    Article Metrics

    Article views(8587) PDF downloads(617) Cited by()
    Proportional views
    Related

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return