动态压力加载/卸载装置dDAC及原位表征技术研究进展

苏磊; 杨国强

doi:10.11858/gywlxb.20210505

动态压力加载/卸载装置dDAC及原位表征技术研究进展

doi: 10.11858/gywlxb.20210505

苏磊^{1, 2,},
杨国强^{1, 3}

1.
中国科学院化学研究所，北京　100190
2.
北京高压科学研究中心，北京　100096
3.
中国科学院大学，北京　100049

基金项目: 国家自然科学基金重大科研仪器专项（21627802）

详细信息

作者简介:
苏　磊（1977－），男，博士，研究员，主要从事高压物理和高压化学研究. E-mail：leisu2050@iccas.ac.cn

中图分类号: O521.3
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出版历程
- 收稿日期: 2021-08-12
- 修回日期: 2021-08-26

Research Progress of Dynamic Pressure Loading/Unloading Device and In-Situ Characterization Technology

SU Lei^{1, 2
,},
YANG Guoqiang^{1, 3}

1.
Institute of Chemistry, Chinese Academy of Sciences, Beijing 100190, China
2.
Center for High Pressure Science and Technology Advanced Research, Beijing 100096, China
3.
University of Chinese Academy of Sciences, Beijing 100049, China

摘要

摘要: 动态压力加载/卸载装置dDAC（Dynamic diamond anvil cell）是近年来备受高压界关注的研究装置之一，可以用来开展亚稳态材料制备、相变动力学、超高压化学等方面研究，在材料学、凝聚态物理学、化学、地学等领域具有重要的应用前景。综述了近年来国内外动态压力加载/卸载装置及原位表征技术的研究进展，详细介绍了一套新型与原位时间分辨光谱测试系统及原位加热/冷却系统相结合的、具有较大加载/卸载速度和较宽压力范围的动态压力加载/卸载装置。该动态压力加载/卸载装置及原位光谱表征系统的建立，将成为新的高压实验研究平台，从而促进高压极端条件下材料新结构和新性能等方面的研究。
- 高压 /
- 金刚石对顶砧 /
- 压力加载 /
- 压力卸载 /
- 光谱学 /
- 高速成像
Abstract: Dynamic pressure loading/unloading device is one of the most important devices which has been paid much attention recently in high pressure research field. It can be effectively used for the preparation of metastable materials, phase transition kinetics, ultra-high pressure chemistry and so on. And it shows many other important application prospects in materials science, condensed state physics, chemistry, and geonomy and so on. In this project, the research progress of dynamic pressure loading/unloading devices and in-situ characterization technology in recent years are summarized, and a novel dynamic pressure loading/unloading device with large pressurization rate and measurable pressure range is developed, which is also combined with both time-resolved spectroscopy test system and in-situ heating/cooling system. It will be a new breakthrough in the research field of high pressure science and technology. And this device can effectively improve the basic research facilities and improve the research on discovering novel structure and functions of materials in the field of high pressure science and technology.
- high pressure /
- diamond anvil cell /
- pressure loading /
- pressure unloading /
- optical spectroscopy /
- high-speed imaging

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图 1 dDAC示意图

Figure 1. Schematic of dDAC

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图 2 dDAC的特征压力加载速度

Figure 2. Characteristic compression rate of dDAC

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图 3 函数信号发生器产生的4种周期性波形

Figure 3. Four types of periodic waveforms generated by function generator

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图 4 时间分辨荧光光谱系统

Figure 4. Time-resolved fluorescent spectroscopy system

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图 5 样品(a)与红宝石(b)的时间分辨荧光光谱

Figure 5. Time-resolved fluorescent spectra of sample (a) and ruby (b)

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图 6 时间分辨拉曼光谱系统

Figure 6. Time-resolved Raman system

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图 7 α-S₈的Raman光谱（曝光时间：1 ms）

Figure 7. Raman spectrum of α-S₈ (exposure time: 1 ms)

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图 8 高速成像系统

Figure 8. High-speed camera system

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图 9 液态硫在动态压力加载过程中的颜色变化（曝光时间：100 μs）

Figure 9. Color change of liquid sulfur captured during pressurization (exposure time: 100 μs)

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参考文献(38)

[1]	HIRAI H, KONDO K I, YOSHIZAWA N, et al. Amorphous diamond from C₆₀ fullerene [J]. Applied Physics Letters, 1994, 64(14): 1797–1799. doi: 10.1063/1.111811
[2]	YANG C, LIU R P, ZHAN Z J, et al. Formation of ZrTiCuNiBe bulk metallic glass by shock-wave quenching [J]. Applied Physics Letters, 2005, 87(5): 051904. doi: 10.1063/1.2005367
[3]	HONG S M, LIU X R, SU L, et al. Rapid compression induced solidification of two amorphous phases of poly (ethylene terephthalate) [J]. Journal of Physics D: Applied Physics, 2006, 39(16): 3684–3688. doi: 10.1088/0022-3727/39/16/024
[4]	JIA R, SHAO C G, SU L, et al. Rapid compression induced solidification of bulk amorphous sulfur [J]. Journal of Physics D: Applied Physics, 2007, 40(12): 3763–3766. doi: 10.1088/0022-3727/40/12/030
[5]	LIU X R, HONG S M, LÜ S J, et al. Preparation of La₆₈A_l10Cu₂₀Co₂ bulk metallic glass by rapid compression [J]. Applied Physics Letters, 2007, 91(8): 081910. doi: 10.1063/1.2773751
[6]	LIU X R, HONG S M. Evidence for a pressure-induced phase transition of amorphous to amorphous in two lanthanide-based bulk metallic glasses [J]. Applied Physics Letters, 2007, 90(25): 251903. doi: 10.1063/1.2749722
[7]	HE D W, ZHANG F X, ZHANG M, et al. Quenching with rapid decompression: a new method for rapid solidification [J]. Applied Physics Letters, 1997, 71(26): 3811–3813. doi: 10.1063/1.120542
[8]	BOEHLER R. Adiabats (∂T/∂P)_s and Grüneisen parameter of NaCl up to 50 kilobars and 800 ℃ [J]. Journal of Geophysical Research: Solid Earth, 1981, 86(B8): 7159–7162. doi: 10.1029/JB086iB08p07159
[9]	BOEHLER R, GETTING I C, KENNEDY G C. Grüneisen parameter of NaCl at high compressions [J]. Journal of Physics and Chemistry of Solids, 1977, 38(3): 233–236. doi: 10.1016/0022-3697(77)90095-6
[10]	王筑明, 谢鸿森, 郭捷, 等. 高压下铝的Grüneisen参数的实验测量 [J]. 高压物理学报, 1998, 12(1): 54–59. doi: 10.11858/gywlxb.1998.01.009 WANG Z M, XIE H S, GUO J, et al. Measurement of Grüneisen parameter of aluminum at high pressure [J]. Chinese Journal of High Pressure Physics, 1998, 12(1): 54–59. doi: 10.11858/gywlxb.1998.01.009
[11]	HONG S M, CHEN L Y, LIU X R, et al. High pressure jump apparatus for measuring Grüneisen parameter of NaCl and studying metastable amorphous phase of Poly (ethylene terephthalate) [J]. Review of Scientific Instruments, 2005, 76(5): 053905. doi: 10.1063/1.1899443
[12]	QUEDNAU J, SCHNEIDER G M. A new high-pressure cell for differential pressure-jump experiments using optical detection [J]. Review of Scientific Instruments, 1989, 60(12): 3685–3687. doi: 10.1063/1.1140475
[13]	SINANIS S, SCHNEIDER G M. Pressure-jump investigations on the kinetics of the isotropic-nematic phase transition of a liquid crystal: time behavior of the scattered and transmitted light intensities for PCH 5 [J]. Berichte der Bunsengesellschaft für Physikalische Chemie, 1998, 102(5): 745–750. doi: 10.1002/bbpc.19981020507
[14]	STEINHART M, KRIECHBAUM M, PRESSL K, et al. High-pressure instrument for small- and wide-angle X-ray scattering. Ⅱ. time-resolved experiments [J]. Review of Scientific Instruments, 1999, 70(2): 1540–1545. doi: 10.1063/1.1149621
[15]	WOENCKHAUS J, KÖHLING R, WINTER R, et al. High pressure-jump apparatus for kinetic studies of protein folding reactions using the small-angle synchrotron X-ray scattering technique [J]. Review of Scientific Instruments, 2000, 71(10): 3895–3899. doi: 10.1063/1.1290508
[16]	WOENCKHAUS J, KÖHLING R, THIYAGARAJAN P, et al. Pressure-jump small-angle X-ray scattering detected kinetics of staphylococcal nuclease folding [J]. Biophysical Journal, 2001, 80(3): 1518–1523. doi: 10.1016/S0006-3495(01)76124-3
[17]	HERBERHOLD H, WINTER R. Temperature- and pressure-induced unfolding and refolding of ubiquitin: a static and kinetic Fourier transform infrared spectroscopy study [J]. Biochemistry, 2002, 41(7): 2396–2401. doi: 10.1021/bi012023b
[18]	HERBERHOLD H, MARCHAL S, LANGE R, et al. Characterization of the pressure-induced intermediate and unfolded state of red-shifted green fluorescent protein: a static and kinetic FTIR, UV/VIS and fluorescence spectroscopy study [J]. Journal of Molecular Biology, 2003, 330(5): 1153–1164. doi: 10.1016/S0022-2836(03)00657-0
[19]	EVANS W J, YOO C S, LEE G W, et al. Dynamic diamond anvil cell (dDAC): a novel device for studying the dynamic-pressure properties of materials [J]. Review of Scientific Instruments, 2007, 78(7): 073904. doi: 10.1063/1.2751409
[20]	LEE W G, EVANS W J, YOO C S. Crystallization of water in a dynamic diamond-anvil cell: evidence for ice Ⅻ-like local order in supercompressed water [J]. Physical Review B, 2006, 74(13): 134112. doi: 10.1103/PhysRevB.74.134112
[21]	LEE G W, EVANS W J, YOO C S. Dynamic pressure-induced dendritic and shock crystal growth of ice Ⅵ [J]. Proceedings of the National Academy of Sciences of the United States of America, 2007, 104(22): 9178–9181. doi: 10.1073/pnas.0609390104
[22]	HABERL B, GUTHRIE M, MALONE B D, et al. Controlled formation of metastable germanium polymorphs [J]. Physical Review B, 2014, 89(14): 144111. doi: 10.1103/PhysRevB.89.144111
[23]	HABERL B, GUTHRIE M, SINOGEIKIN S V, et al. Thermal evolution of the metastable r8 and bc8 polymorphs of silicon [J]. High Pressure Research, 2015, 35(2): 99–116. doi: 10.1080/08957959.2014.1003555
[24]	CHEN J Y, YOO C S. High density amorphous ice at room temperature [J]. Proceedings of the National Academy of Sciences of the United States of America, 2011, 108(19): 7685–7688. doi: 10.1073/pnas.1100752108
[25]	SINOGEIKIN S V, SMITH J S, ROD E, et al. Online remote control systems for static and dynamic compression and decompression using diamond anvil cells [J]. Review of Scientific Instruments, 2015, 86(7): 072209. doi: 10.1063/1.4926892
[26]	KIM Y J, LEE Y H, LEE S, et al. Shock growth of ice crystal near equilibrium melting pressure under dynamic compression [J]. Proceedings of the National Academy of Sciences of the United States of America, 2019, 116(18): 8679–8684. doi: 10.1073/pnas.1818122116
[27]	LIERMANN H P, MORGENROTH W, EHNES A, et al. The extreme conditions beamline at PETRA Ⅲ, DESY: possibilities to conduct time resolved monochromatic diffraction experiments in dynamic and laser heated DAC [C]//International Conference on High Pressure Science and Technology. Tokyo: IOP Publishing, 2010: 012029.
[28]	LIN C L, SMITH J S, SINOGEIKIN S V, et al. Experimental evidence of low-density liquid water upon rapid decompression [J]. Proceedings of the National Academy of Sciences of the United States of America, 2018, 115(9): 2010–2015. doi: 10.1073/pnas.1716310115
[29]	LIN C L, SMITH J S, SINOGEIKIN S V, et al. A metastable liquid melted from a crystalline solid under decompression [J]. Nature Communications, 2017, 8: 14260. doi: 10.1038/ncomms14260
[30]	LIN C L, SMITH J S, SINOGEIKIN S V, et al. Kinetics of the B1-B2 phase transition in KCl under rapid compression [J]. Journal of Applied Physics, 2016, 119(4): 045902. doi: 10.1063/1.4940771
[31]	LIN C L, YONG X, TSE J S, et al. Kinetically controlled two-step amorphization and amorphous-amorphous transition in ice [J]. Physical Review Letters, 2017, 119(13): 135701. doi: 10.1103/PhysRevLett.119.135701
[32]	CHENG H, ZHANG J R, LI Y C, et al. A convenient dynamic loading device for studying kinetics of phase transitions and metastable phases using symmetric diamond anvil cells [J]. High Pressure Research, 2018, 38(1): 32–40. doi: 10.1080/08957959.2017.1396326
[33]	DOU X M, DING K, SUN B Q. Development and application of piezoelectric driving diamond anvil cell device [J]. Review of Scientific Instruments, 2017, 88(12): 123105. doi: 10.1063/1.4996063
[34]	XUE Y Z, WANG H, TAN Q H, et al. Anomalous pressure characteristics of defects in hexagonal boron nitride flakes [J]. ACS Nano, 2018, 12(7): 7127–7133. doi: 10.1021/acsnano.8b02970
[35]	中国科学院化学研究所, 中国科学院大学. 一种用于钻石对顶砧的双向动态加载/卸载的装置和方法: CN110018273A [P]. 2019-07-16.
[36]	中国科学院化学研究所, 中国科学院大学. 一种对钻石对顶砧系统内的样品实现速率可调的加载/卸载的方法: CN111435109A [P]. 2020-07-21.
[37]	ZHANG L, SHI K Y, WANG Y L, et al. Compression rate-dependent crystallization of pyridine [J]. The Journal of Physical Chemistry C, 2021, 125(12): 6983–6989. doi: 10.1021/acs.jpcc.1c01163
[38]	ZHANG L, SHI K Y, WANG Y L, et al. Unraveling the anomalous mechanoluminescence intensity change and pressure-induced red-shift for manganese-doped zinc sulfide [J]. Nano Energy, 2021, 85: 106005. doi: 10.1016/j.nanoen.2021.106005