Introduction of Fourth-Generation High Energy Photon Source HEPS and the Beamlines for High-Pressure Research
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摘要: 作为国家重大科技基础设施“十三五”规划重点建设的项目之一,目前,高能同步辐射光源已经在北京怀柔科学城开始建设,项目目标是建设具有极低发射度、重点覆盖高能区(约300 keV)的第四代同步辐射光源。新的高能光源将为科学研究提供光斑更小、亮度更高、相干性更好的X射线探针。同步辐射光源已经帮助科研人员在高压科学研究的诸多领域取得了丰硕的成果。反过来,应高压研究更高的需求,也在促进同步辐射实验技术的不断发展与进步。本文旨在对高能同步辐射光源首批线站中能够开展高压研究的高压光束线站、吸收谱学线站、高分辨谱学线站和显微成像线站的建设方案进行介绍,一方面有助于用户更好地了解相关设施,另一方面也希望结合用户需求完善后续线站的建设工作,共同推进高压学科在同步辐射领域的发展。Abstract: The High Energy Photon Source (HEPS) located at Huairou’s Science City in Bejing, one of the key projects listed in the “13th Five-year Plan for national major scientific and technological infrastructure”, has been under construction since 2019. HEPS will be a world-leading 4th generation high energy synchrotron radiation source featuring very low emittance, very high brilliance and high X-ray energy (about 300 keV).The new light source will provide X-ray probes with smaller size, higher brightness and better coherence for scientific researches. Synchrotron radiation technology has helped researchers achieve rich results in high-pressure research. In turn, the demand for high-pressure research is also promoting the development of synchrotron radiation experiment technology. In this paper, the design of the beamlines in the HPES phase I for high-pressure research are introduced, including a high-pressure beamline, an X-ray absorption spectroscopy beamline, a hard X-ray high energy resolution spectroscopy beamline and a transmission X-ray microscopy beamline. It is expected to help users well understand the functions of these beamlines, and further promote the development of synchrotron radiation high-pressure research together with the user community via seamless integration of techniques and users’ various requirements for advancing high-pressure science.
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Key words:
- high energy photon source /
- high pressure /
- beamlines
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Energy/
GeVCircumference/
mNumber of
straight sectionsBeam current/
mANatural emittance/
pmradInjection Bunch
number6 1360.4 48 200 34.2 Top-up 680/63 表 2 X射线吸收谱线站的主要设计指标
Table 2. Main parameters of XAS beamline
Energy range/keV Energy resolution(ΔE/E) Flux/(ph·s−1) Spot size /
(μm × μm)Methods 4.8−45 2 × 10−4 Si (111) 5 × 1013@10 keV (non-focus) 0.35 × 0.35 (focus) XAFS/XRD/XRF/FTIR/Mass spectra 4 × 10−5 Si (311) 5 × 1012@10 keV (focus) 0.35 × 0.35 (focus) Time resolution: 25 ms/spectra
Detection limit of trace element > 1×10−7表 3 H2O线站实验方法及技术指标
Table 3. Specification of methods at the H2O beamline
Method Energy range/keV Energy resolution/meV Inject mode Spot size/ (μm × μm) Flux/(ph·s−1) Nuclear resonant scattering 14.4 (57Fe) 2,1 63-bunches 2 × 2 About 1.5 × 1010 X-ray Raman scattering 10 800 680-bunches 3 × 3 About 3 × 1013 -
[1] HEMLEY R J. Effects of high pressure on molecules [J]. Annual Review of Physical Chemistry, 2000, 51: 763–800. doi: 10.1146/annurev.physchem.51.1.763 [2] SHEN G Y, MAO H K. High-pressure studies with x-rays using diamond anvil cells [J]. Reports on Progress in Physics, 2017, 80(1): 016101. doi: 10.1088/1361-6633/80/1/016101 [3] MAO H K, CHEN X J, DING Y, et al. Solids, liquids, and gases under high pressure [J]. Reviews of Modern Physics, 2018, 90: 015007. doi: 10.1103/RevModPhys.90.015007 [4] ASHCROFT N W. Condensed-matter physics: pressure for change in metals [J]. Nature, 2009, 458(7235): 158–159. doi: 10.1038/458158a [5] MCMILLAN P F. Chemistry at high pressure [J]. Chemical Society Reviews, 2006, 35(10): 855–857. doi: 10.1039/B610410J [6] MCMILLAN P F. New materials from high-pressure experiments [J]. Nature Materials, 2002, 1(1): 19–25. doi: 10.1038/nmat716 [7] MAO H K, HEMLEY R J. The high-pressure dimension in earth and planetary science [J]. Proceedings of the National Academy of Sciences of the United States of America, 2007, 104(22): 9114–9115. doi: 10.1073/pnas.0703653104 [8] LI B, JI C, YANG W G, et al. Diamond anvil cell behavior up to 4 mbar [J]. Proceedings of the National Academy of Sciences of the United States of America, 2018, 115(8): 1713–1717. doi: 10.1073/pnas.1721425115 [9] JENEI Z, O’BANNON E F, WEIR S T, et al. Single crystal toroidal diamond anvils for high pressure experiments beyond 5 megabar [J]. Nature Communications, 2018, 9: 3563. doi: 10.1038/s41467-018-06071-x [10] 徐济安, 毕延. 同步辐射X射线光源在高压科学研究中的应用 [J]. 物理, 2012, 41(4): 218–226.XU J A, BI Y. Application of synchrotron radiation X-ray sources in high pressure research [J]. Physics, 2012, 41(4): 218–226. [11] LIU J. High pressure X-ray diffraction techniques with synchrotron radiation [J]. Chinese Physics B, 2016, 25(7): 076106. doi: 10.1088/1674-1056/25/7/076106 [12] 王其武, 刘文汉. X射线吸收精细结构及其应用[M]. 北京: 科学出版社, 1994: 32–35.WANG Q W, LIU W H. X-ray absorption fine structure and it’s application [M]. Beijing: Science Press, 1994: 32–35. [13] CALVIN S. XAFS for everyone [M]. Boca Raton: Taylor & Francis, 2013: 20–21. [14] CHEN J H, DUFFY T S, DOBRZHINETSKAYA L F, et al. Advances in high-pressure technology for geophysical applications [M]. Amsterdam: Elsevier, 2005: 397–411. [15] STERNEMANN C, WILKE M. Spectroscopy of low and intermediate Z elements at extreme conditions: in situ studies of earth materials at pressure and temperature via X-ray raman scattering [J]. High Pressure Research, 2016, 36(3): 275–292. doi: 10.1080/08957959.2016.1198903 [16] 侯琪玥, 敬秋民, 张毅, 等. 基于同步辐射的X射线成像技术在静高压研究中的应用 [J]. 高压物理学报, 2016, 30(6): 537–547. doi: 10.11858/gywlxb.2016.06.016HOU Q Y, JING Q M, ZHANG Y, et al. Applications of synchrotron X-ray imaging techniques in high static pressure researches [J]. Chinese Journal of High Pressure Physics, 2016, 30(6): 537–547. doi: 10.11858/gywlxb.2016.06.016 [17] HETTEL R. The advanced photon source upgrade plan approved [J]. Synchrotron Radiation News, 2019, 32(2): 34–35. doi: 10.1080/08940886.2019.1582289 [18] DIMPER R, REICHERT H, RAIMONDI P, et al. ESRF upgrade programme phase Ⅱ (2015 - 2022) technical design study [R]. France: ESRF, 2014. [19] TANAKA H, ISHIKAWA T, GOTO S, et al. SPring-8 upgrade project [C]//Proceedings of the 7th International Particle Accelerator Conference. Busan: INSPIRE, 2016: 2867–2870. [20] SCHROER C G, AGAPOV I, BREFELD W, et al. PETRA IV: the ultralow-emittance source project at DESY [J]. Journal of Synchrotron Radiation, 2018, 25: 1277–1290. doi: 10.1107/S1600577518008858 [21] JIAO Y, XU G, CUI X H, et al. The HEPS project [J]. Journal of Synchrotron Radiation, 2018, 25: 1611–1618. doi: 10.1107/S1600577518012110 [22] TAO Y. Groundbreaking ceremony at the high energy photon source in Beijing [J]. Synchrotron Radiation News, 2019, 32(5): 40. doi: 10.1080/08940886.2019.1654833 [23] SHEN G, PRAKAPENKA V B, ENG P J, et al. Facilities for high-pressure research with the diamond anvil cell at GSECARS [J]. Journal of Synchrotron Radiation, 2005, 12: 642–649. doi: 10.1107/S0909049505022442 [24] SHEN G Y, CHOW P, XIAO Y M, et al. HPCAT: an integrated high-pressure synchrotron facility at the advanced photon source [J]. High Pressure Research, 2008, 28(3): 145–162. doi: 10.1080/08957950802208571 [25] ANDRAULT D, ANTONANGELI D, DMITRIEV V, et al. Science under extreme conditions of pressures and temperatures at the ESRF [J]. Synchrotron Radiation News, 2013, 26(5): 39–44. doi: 10.1080/08940886.2013.832591 [26] HIRAO N, KAWAGUCHI S I, HIROSE K, et al. New developments in high-pressure X-ray diffraction beamline for diamond anvil cell at SPring-8 [J]. Matter and Radiation at Extremes, 2020, 5(1): 018403. doi: 10.1063/1.5126038 [27] LIERMANN H P, KONÔPKOVÁ Z, MORGENROTH W, et al. The extreme conditions beamline P02.2 and the extreme conditions science infrastructure at PETRA Ⅲ [J]. Journal of Synchrotron Radiation, 2015, 22: 908–924. doi: 10.1107/S1600577515005937 [28] XU W. Nuclear resonant scattering program in China: opportunities and challenges at the high energy photon source in Huairou [J]. Mössbauer Effect Reference and Data Journal, 2017, 40: 213–218. [29] MAO H K, XU J, STRUZHKIN V V, et al. Phonon density of states of iron up to 153 gigapascals [J]. Science, 2001, 292(5518): 914–916. doi: 10.1126/science.1057670 [30] LIU J, HU Q Y, KIM D Y, et al. Hydrogen-bearing iron peroxide and the origin of ultralow-velocity zones [J]. Nature, 2017, 551(7681): 494–497. doi: 10.1038/nature24461 [31] KUPENKO I, APRILIS G, VASIUKOV D M, et al. Magnetism in cold subducting slabs at mantle transition zone depths [J]. Nature, 2019, 570(7759): 102–106. doi: 10.1038/s41586-019-1254-8 [32] WU J J, LIN J F, WANG X C, et al. Pressure-decoupled magnetic and structural transitions of the parent compound of iron-based 122 superconductors BaFe2As2 [J]. Proceedings of the National Academy of Sciences of the United States of America, 2013, 110(43): 17263–17266. doi: 10.1073/pnas.1310286110 [33] TROYAN I, GAVRILIUK A, RÜFFER R, et al. Observation of superconductivity in hydrogen sulfide from nuclear resonant scattering [J]. Science, 2016, 351(6279): 1303–1306. doi: 10.1126/science.aac8176 [34] BI W, SOUZA-NETO N M, HASKEL D, et al. Synchrotron x-ray spectroscopy studies of valence and magnetic state in europium metal to extreme pressures [J]. Physical Review B, 2012, 85(20): 205134. doi: 10.1103/PhysRevB.85.205134 [35] BI W, LIM J, FABBRIS G, et al. Magnetism of europium under extreme pressures [J]. Physical Review B, 2016, 93(18): 184424. doi: 10.1103/PhysRevB.93.184424 [36] CAI Y Q, MAO H K, CHOW P C, et al. Ordering of hydrogen bonds in high-pressure low-temperature H2O [J]. Physical Review Letters, 2005, 94(2): 025502. doi: 10.1103/PhysRevLett.94.025502 [37] SHIEH S R, JARRIGE I, WU M, et al. Electronic structure of carbon dioxide under pressure and insights into the molecular-to-nonmolecular transition [J]. Proceedings of the National Academy of Sciences of the United States of America, 2013, 110(46): 18402–18406. doi: 10.1073/pnas.1305116110 [38] LEE S K, KIM Y H, YI Y S, et al. Oxygen quadclusters in SiO2 glass above megabar pressures up to 160 GPa revealed by X-ray Raman scattering [J]. Physical Review Letters, 2019, 123(23): 235701. doi: 10.1103/PhysRevLett.123.235701 [39] CHEN B J, PARSCHKE E M, CHEN W C, et al. Probing cerium 4f states across the volume collapse transition by X-ray Raman scattering [J]. The Journal of Physical Chemistry Letters, 2019, 10(24): 7890–7897. doi: 10.1021/acs.jpclett.9b02819 [40] MEIRER F, CABANA J, LIU Y, et al. Three-dimensional imaging of chemical phase transformations at the nanoscale with full-field transmission X-ray microscopy [J]. Journal of Synchrotron Radiation, 2011, 18(5): 773–781. doi: 10.1107/S0909049511019364 [41] LIU H Z, WANG L H, XIAO X H, et al. Anomalous high-pressure behavior of amorphous selenium from synchrotron x-ray diffraction and microtomography [J]. Proceedings of the National Academy of Sciences of the United States of America, 2008, 105(36): 13229–13234. doi: 10.1073/pnas.0806857105 [42] XIAO X H, LIU H Z, WANG L H, et al. Density measurement of samples under high pressure using synchrotron microtomography and diamond anvil cell techniques [J]. Journal of Synchrotron Radiation, 2010, 17(3): 360–366. doi: 10.1107/S0909049510008502 [43] WANG J Y, YANG W G, WANG S, et al. High pressure nano-tomography using an iterative method [J]. Journal of Applied Physics, 2012, 111(11): 112626. doi: 10.1063/1.4726249 [44] LIN Y, ZENG Q S, YANG W G, et al. Pressure-induced densification in GeO2 glass: a transmission x-ray microscopy study [J]. Applied Physics Letters, 2013, 103(26): 261909. doi: 10.1063/1.4860993 [45] ZENG Q S, KONO Y, LIN Y, et al. Universal fractional noncubic power law for density of metallic glasses [J]. Physical Review Letters, 2014, 112(18): 185502. doi: 10.1103/PhysRevLett.112.185502 [46] KATAYAMA Y, INAMURA Y, MIZUTANI T, et al. Macroscopic separation of dense fluid phase and liquid phase of phosphorus [J]. Science, 2004, 306(5697): 848–851. doi: 10.1126/science.1102735 [47] LIU Y J, WANG J Y, AZUMA M, et al. Five-dimensional visualization of phase transition in BiNiO3 under high pressure [J]. Applied Physics Letters, 2014, 104(4): 043108. doi: 10.1063/1.4863229 [48] ZHU W L, GAETANI G A, FUSSEIS F, et al. Microtomography of partially molten rocks: three-dimensional melt distribution in mantle peridotite [J]. Science, 2011, 332(6025): 88–91. doi: 10.1126/science.1202221 [49] SHI C Y, ZHANG L, YANG W G, et al. Formation of an interconnected network of iron melt at Earth’s lower mantle conditions [J]. Nature Geoscience, 2013, 6(11): 971–975. doi: 10.1038/ngeo1956 [50] YUAN Q X, ZHANG K, HUANG W X, et al. Conceptual design of TXM beamline at high energy photon source [J]. AIP Conference Proceedings, 2019, 2054(1): 050002. doi: 10.1063/1.5084620