磁驱动斜波加载下铋的Ⅰ-Ⅱ-Ⅲ相变实验

种涛; 谭福利; 王桂吉; 赵剑衡; 唐志平

doi:10.11858/gywlxb.20180511

磁驱动斜波加载下铋的Ⅰ-Ⅱ-Ⅲ相变实验

doi: 10.11858/gywlxb.20180511

种涛^{1, 2,},
谭福利²,
王桂吉²,
赵剑衡^2,*, ,,
唐志平¹

1.
中国科学技术大学近代力学系, 安徽合肥 230027
2.
中国工程物理研究院流体物理研究所, 四川绵阳 621999

基金项目:

国家自然科学基金委重大科研仪器设备专项 11327803

四川省青年科技创新研究团队专项计划项目 2016TD0022

科学挑战专题 JCKY2016212A501

详细信息

作者简介:
种涛(1986-), 男, 博士, 主要从事动高压加载技术和材料动力学行为研究.E-mail:maoda318@163.com

通讯作者:
赵剑衡(1969-), 男, 博士, 研究员, 博士生导师, 主要从事强激光破坏机理、爆轰物理、冲击动力学、超高速发射和超高压力加载技术研究.E-mail:jianh_zhao@caep.cn

中图分类号: O521.2
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出版历程
- 收稿日期: 2018-01-29
- 修回日期: 2018-03-19

Ⅰ-Ⅱ-Ⅲ Phase Transition of Bismuth under Magnetically Driven Ramp Wave Loading

CHONG Tao^{1, 2
,},
TAN Fuli²,
WANG Guiji²,
ZHAO Jianheng^{2,*
, ,},
TANG Zhiping¹

1.
Department of Modern Mechanics, University of Science and Technology of China, Hefei 230027, China
2.
Institute of Fluid Physics, CAEP, Mianyang 621999, China

摘要

摘要: 设计了一套与磁驱动斜波加载实验装置CQ-4配套的样品预设温度系统，温度范围为室温至180℃。利用此装置联合双源光外差测速系统，完成了不同初始温度下铋的斜波压缩相变实验，并在单发实验中获得了同时含有Ⅰ-Ⅱ和Ⅱ-Ⅲ两次相变信息的速度剖面。实验结果显示，随着铋的初始温度从室温提高到148℃，Ⅰ-Ⅱ相变和Ⅱ-Ⅲ相变起始对应的特征拐点速度分别从251.6和275.7 m/s下降到239.4和259.7 m/s。
- 斜波压缩 /
- 初始温度 /
- 相变 /
- 铋 /
- 速度剖面
Abstract: In this study, we developed a sample pre-heating system with the temperature range from room temperature to 180℃, matching with the magnetically driven apparatus CQ-4.The ramp wave compression experiments of bismuth under different initial temperatures (25-148℃) were carried out, using this pre-heating system on CQ-4.The free surface velocity profiles, measured by a dual laser heterodyne velocimetry, show clearly two phase transitions of bismuth during the compression.Furthermore, with the initial temperature increasing from room temperature to 148℃, the characteristic free surface velocities corresponding to the onsets of Ⅰ-Ⅱ and Ⅱ-Ⅲ phase transition decreases from 251.6 and 275.7 m/s to 239.4 and 259.7 m/s, respectively.
- ramp wave compression /
- initial temperature /
- phase transition /
- bismuth /
- velocity profile

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图 1 磁压加载原理及实验布局

Figure 1. Schematic of the magnetically driven ramp wave loading experiments

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图 2 升温实验负载区布局

Figure 2. Layout of loading area in heating experiment

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图 3 铋样品自由面速度剖面及相图

Figure 3. Free surface velocities and phase diagram of bismuth

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表 1 实验条件

Table 1. Experimental conditions

Exp.No.	T₀/℃	Position	Material	Dimension
Shot 342	100	Plate Sample Bedding	Al Bi Sapphire	10.0 mm×30.0 mm×0.971 mm ∅7.9 mm×1.178 mm 10.0 mm×28.0 mm×0.800 mm
Shot 343	148	Plate Sample Bedding	Al Bi Sapphire	10.0 mm×30.0 mm×1.001 mm ∅7.9 mm×1.131 mm 10.0 mm×28.0 mm×0.798 mm
Shot 344	25	Plate Sample Bedding	Al Bi Sapphire	10.0 mm×30.0 mm×0.983 mm ∅7.9 mm×1.150 mm 10.0 mm×28.0 mm×0.796 mm

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表 2 两次相变对应的特征速度和压力

Table 2. Characteristic free surface velocities and pressures corresponding to the two phase transitions

Exp.No.	T₀/℃	Characteristic velocity/(m·s^-1)		Phase transition pressure/GPa
Exp.No.	T₀/℃	Ⅰ-Ⅱ	Ⅱ-Ⅲ	Ⅰ-Ⅱ	Ⅱ-Ⅲ
Shot 344	25	251.6	275.7	2.53	2.81
Shot 342	100	244.9	266.0	2.45	2.69
Shot 343	148	239.4	259.7	2.39	2.62

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参考文献(27)

[1]	BRIDGMAN P W.Polymorphism, principally of the elements, up to 50000 kg/cm²[J].Physical Review, 1935, 48(11):893. doi: 10.1103/PhysRev.48.893
[2]	BRIDGMAN P W.The resistance of 72 elements, alloys and compounds to 100000 kg/cm²[J].Proceedings of the American Academy of Arts and Sciences, 1952, 81(4):165-251. doi: 10.2307/20023677
[3]	BRIDGMAN P W.Compressions and polymorphic transitions of seventeen elements to 100000 kg/cm²[J].Physical Review, 1941, 60(4):351. doi: 10.1103/PhysRev.60.351
[4]	BUNDY F P.Phase diagram of bismuth to 130000 kg/cm², 500℃[J].Physical Review, 1958, 110(2):314. doi: 10.1103/PhysRev.110.314
[5]	HOMAN C G.Phase diagram of Bi up to 140 kbars[J].Journal of Physics and Chemistry of Solids, 1975, 36(11):1249-1254. doi: 10.1016/0022-3697(75)90199-7
[6]	KOSSOWSKY R.Observations of the Bi Ⅲ-Ⅳ and Bi Ⅳ-Ⅴ transitions by measurements[J].Transactions of the Metallurgical Society of AIME, 1966, 236(12):1746-1748. http://www.cjcu.jlu.edu.cn/EN/volumn/volumn_1262.shtml
[7]	PHILLIPS D, JURA G.The electrical resistance of bismuth from 25 to 90 kbars[J].Transactions of the Metallurgical Society of AIME, 1967, 239(1):120-121.
[8]	MCMAHON M I, DEGTYAREVA O, NELMES R J, et al.Incommensurate modulations of Bi-Ⅲ and Sb-Ⅱ[J].Physical Review B, 2007, 75(18):184114. doi: 10.1103/PhysRevB.75.184114
[9]	MCMAHON M I, DEGTYAREVA O, NELMES R J.Ba-Ⅳ-type incommensurate crystal structure in group-Ⅴ metals[J].Physical Review Letters, 2000, 85(23):4896-4899. doi: 10.1103/PhysRevLett.85.4896
[10]	DEGTYAREVA O, MCMAHON M I, NELMES R J.High-pressure structural studies of group-15 elements[J].High Pressure Research, 2004, 24(3):319-356. doi: 10.1080/08957950412331281057
[11]	DUFF R E, MINSHALL F S.Investigation of a shock-induced transition in bismuth[J].Physical Review, 1957, 108(5):1207. doi: 10.1103/PhysRev.108.1207
[12]	LARSON D B.A shock-induced phase transformation in bismuth[J].Journal of Applied Physics, 1967, 38(4):1541-1546. doi: 10.1063/1.1709720
[13]	ASAY J R.Shock-induced melting in bismuth[J].Journal of Applied Physics, 1974, 45(10):4441-4452. doi: 10.1063/1.1663070
[14]	谭叶. 金属铋的冲击相变与多相物态方程研究[D]. 绵阳: 中国工程物理研究院, 2011. http://www.wanfangdata.com.cn/details/detail.do?_type=degree&id=Y2907332
[15]	种涛, 王桂吉, 谭福利, 等.磁驱动准等熵压缩下铁的相变[J].中国科学:物理学力学天文学, 2014, 44(6):630-636. https://www.researchgate.net/profile/Guiji_Wang/publication/274232992_Phase_transition_of_iron_under_magnetically_driven_quasi-isentropic_compression/links/556c3c8e08aefcb861d63387.pdf?inViewer=0&pdfJsDownload=0&origin=publication_detail CHONG T, WANG G J, TAN F L, et al.Phase transition of iron under magnetically driven quasi-isentropic compression[J].Scientia Sinica:Physica, Mechanica & Astronomica, 2014, 44(6):630-636. https://www.researchgate.net/profile/Guiji_Wang/publication/274232992_Phase_transition_of_iron_under_magnetically_driven_quasi-isentropic_compression/links/556c3c8e08aefcb861d63387.pdf?inViewer=0&pdfJsDownload=0&origin=publication_detail
[16]	RIGG P A, GREEFF C W, KNUDSON M D, et al.Influence of impurities on the α to ω phase transition in zirconium under dynamic loading conditions[J].Journal of Applied Physics, 2009, 106(12):123532. doi: 10.1063/1.3267325
[17]	BASTEA M, BASTEA S, EMIG J A, et al.Kinetics of propagating phase transformation in compressed bismuth[J].Physical Review B, 2005, 71(18):180101. doi: 10.1103/PhysRevB.71.180101
[18]	SMITH R F, EGGERT J H, SACULLA M D, et al.Ultrafast dynamic compression technique to study the kinetics of phase transformations in bismuth[J].Physical Review Letters, 2008, 101(6):065701. doi: 10.1103/PhysRevLett.101.065701
[19]	HU J, ICHIYANAGI K, DOKI T, et al.Complex structural dynamics of bismuth under laser-driven compression[J].Applied Physics Letters, 2013, 103(16):161904. doi: 10.1063/1.4825276
[20]	NGUYEN J H, ORLIKOWSKI D, STREITZ F H, et al.Specifically prescribed dynamic thermodynamic paths and resolidification experiments[J].AIP Conference Proceedings, 2004, 706(1):1225-1230. https://core.ac.uk/display/71300822
[21]	WANG G J, LUO B Q, ZHANG X P, et al.A 4 MA, 500 ns pulsed power generator CQ-4 for characterization of material behaviors under ramp wave loading[J].Review of Scientific Instruments, 2013, 84(1):015117. doi: 10.1063/1.4788935
[22]	HALL C A, ASAY J R, KNUDSON M D, et al.Experimental configuration for isentropic compression of solids using pulsed magnetic loading[J].Review of Scientific Instruments, 2001, 72(9):3587-3595. doi: 10.1063/1.1394178
[23]	种涛. 磁驱动准等熵压缩下锆的相变特性初步研究及电磁膨胀环模拟[D]. 绵阳: 中国工程物理研究院, 2012. http://cdmd.cnki.com.cn/Article/CDMD-82818-1012499410.htm
[24]	罗斌强, 谭福利, 赵剑衡. 磁驱动准等熵加载实验中加载压力均匀性分析[C]//第九届全国爆炸力学学术会议论文集. 西宁, 2012.
[25]	陶天炯, 翁继东, 王翔.一种双源光外差测速技术[J].光电工程, 2011, 38(10):39-45. doi: 10.3969/j.issn.1003-501X.2011.10.007 TAO T J, WENG J D, WANG X.A dual laser heterodyne velocimetry[J].Opto-Electronic Engineering, 2011, 38(10):39-45. doi: 10.3969/j.issn.1003-501X.2011.10.007
[26]	罗斌强, 张红平, 种涛, 等.磁驱动斜波压缩实验结果的不确定度分析[J].高压物理学报, 2017, 31(3):295-300. doi: 10.11858/gywlxb.2017.03.011 LUO B Q, ZHANG H P, CHONG T, et al.Experimental uncertainty analysis of magnetically driven ramp wave compression[J].Chinese Journal of High Pressure Physics, 2017, 31(3):295-300. doi: 10.11858/gywlxb.2017.03.011
[27]	唐志平.冲击相变[M].北京:科学出版社, 2008.